Work Areas 20 bench hoods Four 6-foot walk-in hoods One 12-foot walk-in hood 180-square-foot reactor booth

Equipment

• Reactors and work-up stations to 72L
• 10L Rotary evaporator
• 20L Rotary evaporator
• Photochemical reactors to 72L
• Parr hydrogenator to 2.5L
• Parr pressure reactor 19L/2,000 psi
• Ozone generator
• Fractional distillation equipment
• (2) Kugelrohr distillation apparatus
• (2) 12L spinning band stills (30 theoretical plates)
• Prep MPLC systems (up to 24L silica at 600 mL/min)
• Wiped-Film Evaporator (0.06m2, 0.04-5 Kg/hr)
• Centrifuge (14", 7L, 2500G)
• Ultrapure water system
• Reaction block for combinatorial synthesis

• NMR, 400 MHz (¹H, ¹³C, ¹⁹F, ³¹P)
• LC/MS (APCi, ESI)
• GCs (FID)
• LCs (UV, RI, DAD)
• FT-IR
• Karl Fischer titrator